USGS OFR-02-94 Table 5, Method 4

Table 5. Stream sampling sites analyzed for selected organic wastewater compounds (Method 4) in 1999 and 2000
[All concentrations are in micrograms per liter. <, less than indicated detected limit; E, estimated; --, data not collected; Number in parentheses is the Chemical Abstracts Registry Number]

Site code	Date (month-day-year)	Time (24-hour)	Type of sample	1,4-dichlorobenzene (106-46-7)	2,6-di-tert-butyl-phenol (128-39-2)	2,6-di-tert-p-benzoquinone (719-22-2)	3-tert-butyl-4-hydroxy anisole (25013-16-5)	4-methyl phenol (106-44-5)	4-nonylphenol(84852-15-3)	4-nonylphenol monoethoxylate (NA)	4-nonylphenol diethoxylate (NA)
AR02	05-02-99	1630	regular	--	--	--	--	--	--	--	--
AR06	05-04-99	2050	do.	<0.030	<0.090	0.46	<0.120	<0.030	<.500	<1.000	<1.100
AZ01	06-29-00	1115	do.	<.030	<.080	<.500	<.120	<.060	E4	E2	E2
AZ02	06-27-00	1625	do.	.37	<.080	<.500	<.120	.43	E4	E5	E9
AZ03	06-29-00	0710	do.	.63	<.080	<.500	<.120	<.060	E40	E10	E6
AZ04	06-27-00	1035	do.	.31	<.090	.13	<.120	<.030	E.4	<1.000	<1.100
CA01	05-18-00	1130	do.	<.030	<.090	<.070	<.120	<.030	<.500	<1.000	<1.100
CA02	06-28-00	1300	do.	E.01	<.090	E.04	<.120	<.030	<.500	E.2	E.2
CA03	08-16-00	1700	do.	<.040	<.150	E.4	<.120	E.05	E.7	E2	E4
CA04	08-09-00	1700	do.	.10	<.150	<.500	<.120	.03	E.4	E1	E1
CA05	04-15-99	1700	do.	--	--	--	--	--	--	--	--
CA06	04-11-99	0715	do.	<.030	<.090	<.070	<.120	E.08	<.500	<1.000	<1.100
CA07	09-21-99	1110	do.	<.030	<.090	<.070	<.100	<.030	<.500	<.800	<1.000
CA08	09-21-99	1600	do.	<.030	<.090	<.070	<.100	<.030	<.500	<.800	<1.000
CA09	09-22-99	1120	do.	<.030	<.090	<.070	<.100	<.030	<.500	<.800	<1.000
CA10	09-22-99	1320	do.	<.030	<.090	<.070	<.100	<.030	<.500	<.800	<1.000
CO01	04-21-99	1250	do.	.71	<.090	<.070	E.2	<.030	E10	E20	<1.100
DE01	05-23-99	1130	do.	<.030	<.090	<.070	<.120	<.030	<.500	<1.000	<1.100
DE01	05-23-99	1140	duplicate	<.030	E.04	<.070	<.120	<.030	E.5	E.1	<1.100
FL01	08-28-00	1215	regular	.21	<.150	<.500	<.120	E.04	E.3	E.4	E.8
FL02	08-23-00	1215	do.	<.040	<.150	<.500	<.120	E.04	E.3	E.9	E.4
GA01	05-26-99	1400	do.	--	--	--	--	--	--	--	--
GA02	05-25-99	1130	do.	--	--	--	--	--	--	--	--
GA03	05-25-99	1030	do.	--	--	--	--	--	--	--	--
GA04	05-25-99	0840	do.	<.030	<.090	<.070	<.120	<.030	<.500	E.32	E.4
GA05	05-26-99	1130	do.	--	--	--	--	--	--	--	--
GA06	05-24-99	1215	do.	--	--	--	--	--	--	--	--
GA07	05-31-00	1115	do.	E.02	<.090	<.070	<.120	<.030	<.500	<1.000	E1
IA01	09-13-00	1600	do.	<.030	<.080	<.500	<.120	<.040	E.7	<1.000	<1.100
IA02	09-12-00	1200	do.	<.030	<.080	<.500	<.120	<.060	<.500	<1.000	<1.100
IA04	09-11-00	1700	do.	<.030	<.080	<.500	<.120	<.040	E.9	E1	<1.100
IA05	04-05-99	1445	do.	--	--	--	--	--	--	--	--
IA07	04-08-99	1000	do.	--	--	--	--	--	--	--	--
IA08	04-06-99	0935	do.	--	--	--	--	--	--	--	--
IA09	04-06-99	1245	do.	<.030	<.090	<.070	<.120	E.02	E.6	E.3	E.04
IA10	04-04-99	2000	do.	--	--	--	--	--	--	--	--
IA11	04-03-99	1855	do.	--	--	--	--	--	--	--	--
IA12	04-03-99	1245	do.	--	--	--	--	--	--	--	--
ID01	08-14-00	1110	do.	--	--	--	--	--	--	--	--
ID02	08-15-00	1250	do.	.22	<.150	<.500	<.120	<.060	E.3	<1.000	<1.100
ID03	08-16-00	1222	do.	.26	<.150	<.500	<.120	<.060	E.4	<1.000	<1.100
ID04	05-17-00	1215	do.	<.030	<.090	<.070	<.120	<.030	<.500	<1.000	<1.100
IL01	05-13-99	1300	do.	--	--	--	--	--	--	--	--
IL02	05-17-99	1420	do.	--	--	--	--	--	--	--	--
IL03	09-06-00	1050	do.	<.030	<.080	<.500	<.120	<.040	E.8	<1.000	<1.100
IL04	09-06-00	0940	do.	<.030	<.080	<.500	<.120	<.040	E.8	<1.000	<1.100
IL05	05-20-99	0810	do.	.17	<.090	<.070	<.120	.07	E3	E1	E.7
IL06	05-17-99	1230	do.	--	--	--	--	--	--	--	--
IL07	05-13-99	1710	do.	--	--	--	--	--	--	--	--
LA01	04-19-99	1130	do.	4.3	<.090	<.070	<.120	<.030	E1	<1.000	<1.100
MA01	05-12-99	0840	do.	--	--	--	--	--	--	--	--
MA02	07-25-00	0630	do.	<.030	<.080	<.500	<.120	<.040	<.500	E1	<1.100
MA03	07-25-00	0750	blank	<.030	<.080	<.500	<.120	<.040	<.500	<1.000	<1.100
MA03	07-25-00	0800	regular	<.030	<.080	<.500	<.120	<.040	<.500	E1	<1.100
MA03	07-25-00	0810	duplicate	<.030	<.080	<.500	<.120	<.040	<.500	<1.000	<1.100
MA04	07-25-00	0900	regular	<.030	<.080	<.500	<.120	<.040	<.500	E1	<1.100
MA05	07-25-00	1100	do.	<.030	<.080	<.500	<.120	<.040	<.500	E1	<1.100
MA06	07-25-00	1010	do.	<.030	<.080	<.500	<.120	E.3	<.500	E2	E5
MA07	07-25-00	1130	do.	<.030	<.080	<.500	<.120	<.040	E1	<1.000	<1.100
MD01	09-17-99	0930	do.	--	--	--	--	--	--	--	--
MD02	05-19-99	1710	do.	--	--	--	--	--	--	--	--
MI01	06-15-99	1030	do.	--	--	--	--	--	--	--	--
MI02	06-15-99	1430	do.	--	--	--	--	--	--	--	--
MI03	06-16-99	1045	do.	0.06	E.1	E.06	<.120	<.030	<.500	<1.000	<1.100
MN03	10-03-00	1105	blank	<.040	<.150	<.500	<.120	<.060	E.5	<1.000	<1.100
MN03	10-03-00	1115	regular	<.040	<.150	<.500	<.120	<.060	E.6	<1.000	<1.100
MN04	10-02-00	1210	do.	<.040	<.150	<.500	<.120	E.03	E.5	<1.000	<1.100
MO01	05-06-99	1130	do.	<.030	<.090	<.070	<.120	<.030	E2	E.8	E.6
MO02	04-29-99	1245	do.	E.03	<.090	.14	E.1	.13	E1	E2	E4
MO03	04-30-99	0830	do.	E.03	<.090	<.070	<.120	<.030	E.7	E1	E2
MO04	04-30-99	1300	do.	.09	<.090	<.070	<.120	<.030	E.9	E.7	E1
MO05	05-15-99	1315	do.	<.030	<.090	<.070	<.120	E.02	<.500	<1.000	<1.100
MO06	04-07-99	0845	do.	<.030	<.090	<.070	<.120	<.030	<.500	<1.000	<1.100
MO07	04-05-99	1530	do.	--	--	--	--	--	--	--	--
MO08	04-07-99	0840	do.	--	--	--	--	--	--	--	--
MT01	03-16-00	1040	do.	<.030	<.090	<.070	<.120	<.030	<.500	E1	E.8
MT02	03-16-00	1400	do.	<.030	<.090	<.070	<.120	<.030	E5	E10	E9
MT03	03-17-00	1100	do.	<.030	<.090	<.070	<.120	<.030	E.5	E2	E.7
MT04	03-06-00	1400	do.	<.030	<.090	<.070	<.120	<.030	E1	<1.000	<1.100
MT05	03-22-00	1130	do.	<.030	<.090	<.070	<.120	<.030	<.500	<1.000	<1.100
NC01	05-06-99	1015	do.	--	--	--	--	--	--	--	--
NC02	05-06-99	1230	do.	--	--	--	--	--	--	--	--
NC03	05-06-99	1430	do.	--	--	--	--	--	--	--	--
NC04	05-06-99	1545	do.	--	--	--	--	--	--	--	--
NC05	05-13-99	1245	do.	--	--	--	--	--	--	--	--
NE01	06-24-99	1330	do.	--	--	--	--	--	--	--	--
NE02	06-15-99	1730	do.	<.030	<.090	<.070	<.120	<.030	<.500	<1.000	<1.100
NE03	06-14-99	1600	do.	<.030	E.05	<.070	<.120	<.030	<.500	<1.000	<1.100
NE04	06-15-99	1700	do.	--	--	--	--	--	--	--	--
NE05	06-03-99	1230	do.	--	--	--	--	--	--	--	--
NE06	06-04-99	1030	do.	--	--	--	--	--	--	--	--
NE07	06-17-99	1130	do.	--	--	--	--	--	--	--	--
NJ01	06-01-99	1020	do.	--	--	--	--	--	--	--	--
NJ02	08-15-00	1300	do.	<.030	<.080	<.500	<.120	<.060	E3	E2	<1.100
NJ03	08-17-00	1040	do.	<.040	<.150	<.500	<.120	<.060	E.3	<1.000	<1.100
NJ04	05-27-99	1120	do.	--	--	--	--	--	--	--	--
NY01	03-28-00	1310	do.	<.040	<.150	<.500	<.120	.12	E.4	<1.000	<1.100
NY02	08-08-00	1150	do.	<.040	<.150	<.500	<.120	<.060	<.700	<1.000	<1.100
NY03	08-23-00	1340	do.	<.040	<.150	<.500	<.120	.44	E7	E9	E2
NY04	08-08-00	1100	do.	<.040	<.150	<.500	<.120	<.060	<.700	<1.000	<1.100
NY05	08-08-00	1300	do.	<.040	<.150	<.500	<.120	<.060	E.3	<1.000	<1.100
NY06	08-08-00	1500	do.	<.040	<.150	<.500	<.120	<.060	<.700	<1.000	<1.100
NY07	08-08-00	1410	do.	<.040	<.150	<.500	<.120	E.06	<.700	<1.000	<1.100
NY07	08-08-00	1415	duplicate	<.040	<.150	<.500	<.120	E.05	E.3	E.6	<1.100
NY08	08-30-00	1430	regular	<.030	<.080	<.500	<.120	E.04	E2	E5	E5
NY09	08-10-00	1215	do.	<.040	<.150	<.500	<.120	<.060	E.2	<1.000	E.7
NY10	08-10-00	1120	do.	.06	<.150	<.500	<.120	.06	E6	E8	E8
NY11	08-10-00	1609	blank	<.040	<.150	<.500	<.120	<.060	<.700	<1.000	<1.100
NY11	08-10-00	1625	regular	<.040	<.150	<.500	<.120	<.060	<.700	<1.000	<1.100
NY12	08-10-00	1515	do.	<.040	<.150	<.500	<.120	<.060	E.3	E.6	E.8
OH01	10-05-00	1110	do.	<.040	<.150	<.500	<.120	E.04	E.6	E3	E3
OH02	05-24-99	1015	do.	E.03	<.090	.08	<.120	<.030	E2	E1	E2
OH03	05-06-99	1045	do.	--	--	--	--	--	--	--	--
OH04	05-06-99	1340	do.	--	--	--	--	--	--	--	--
OH05	07-13-00	1130	do.	<.030	<.080	<.500	<.120	<.060	<.500	<1.000	<1.100
OH06	05-24-99	1245	do.	--	--	--	--	--	--	--	--
OH07	06-02-99	1145	do.	--	--	--	--	--	--	--	--
OH08	06-14-99	1120	do.	<.030	E.06	<.070	<.120	<.030	<.500	<1.000	<1.100
OK01	05-13-99	1315	do.	<.030	<.090	<.070	<.120	<.030	E.7	E.07	<1.100
OK03	05-03-99	1045	do.	<.030	<.090	<.070	<.120	<.030	E1	E.5	E.3
OK04	05-24-99	1300	do.	<.030	<.090	<.070	<.120	<.030	<.500	<1.000	<1.100
OR02	07-10-00	1400	do.	<.030	<.090	<.070	<.120	<.030	<.500	<1.000	<1.100
OR03	06-03-00	1030	do.	.06	<.090	<.070	<.120	<.030	<.500	E.5	E.8
OR04	07-24-00	1130	do.	<.030	<.080	<.500	<.120	<.040	E.4	E1	<1.100
PA01	05-24-99	1030	do.	--	--	--	--	--	--	--	--
PA02	06-08-99	1120	do.	--	--	--	--	--	--	--	--
PA03	05-27-99	1520	do.	--	--	--	--	--	--	--	--
PA04	05-27-99	1000	do.	<.030	<.090	<.070	<.120	<.030	E.6	E.2	<1.100
PA05	05-27-99	1150	do.	--	--	--	--	--	--	--	--
TX01	08-09-99	0830	do.	.08	<.090	.22	<.100	<.030	E1	E.9	E.6
UT01	06-14-99	1140	do.	E.01	<.090	<.070	<.120	<.030	<.500	<1.000	<1.100
VA01	08-01-00	1500	do.	<.030	<.080	<.500	<.120	.54	<.500	<1.000	<1.100
WA01	07-19-00	0930	do.	<.030	<.080	<.500	<.120	<.040	<.500	<1.000	<1.100
WA02	05-18-99	1530	do.	--	--	--	--	--	--	--	--
WA03	05-14-99	1530	do.	<.030	<.090	<.070	<.120	<.030	<.500	<1.000	<1.100
WA04	05-06-99	1050	do.	--	--	--	--	--	--	--	--
WA05	05-14-99	1200	do.	--	--	--	--	--	--	--	--
WA06	03-29-00	1000	do.	E.01	<.090	<.070	<.120	E.02	<.500	E.6	E.5
WI01	04-23-99	0955	do.	--	--	--	--	--	--	--	--
WI02	04-23-99	0910	do.	<.030	<.090	<.070	<.120	.04	<.500	<1.000	<1.100
WI03	05-17-99	1230	do.	--	--	--	--	--	--	--	--
WI04	04-23-99	1450	do.	--	--	--	--	--	--	--	--
WI05	04-23-99	1115	do.	--	--	--	--	--	--	--	--
WI06	04-23-99	1330	do.	--	--	--	--	--	--	--	--
WI07	04-23-99	0820	do.	--	--	--	--	--	--	--	--

Table 5. Selected compounds, Method 4 - Continued

Site code	Date (month-day-year)	Time (24-hour)	Type of sample	4-octylphenol monoethoxylate (26636-32-8)	4-octylphenol diethoxylate (26636-32-8)	5-methyl-1H-benzo-triazle (136-85-6)	Aceto-phenone (98-86-2)	Anthra-cene (120-12-7)	Benzo (a) pyrene (50-32-8)	Bis (2-ethylhexyl) adipate (103-23-1)	Bis (2-ethylhexyl) phthalate (117-81-7)	Bis-phenol A (80-05-7)
AR02	05-02-99	1630	regular	--	--	--	--	--	--	--	--	--
AR06	05-04-99	2050	do.	<0.100	<0.200	--	<0.100	0.03	E.02	E3	<2.000	<0.090
AZ01	06-29-00	1115	do.	E.1	<.200	.39	<.220	<.060	<.050	<2.000	<2.500	12
AZ02	06-27-00	1625	do.	E.4	E.1	2.4	<.220	<.060	<.050	<2.000	<2.500	5.2
AZ03	06-29-00	0710	do.	E1	<.200	2.1	.28	<.060	<.050	<2.000	<2.500	.40
AZ04	06-27-00	1035	do.	<.100	<.200	.54	<.100	<.050	<.050	<1.500	<2.000	E.06
CA01	05-18-00	1130	do.	<.100	<.200	<.100	<.100	<.050	<.050	<1.500	<2.000	<.090
CA02	06-28-00	1300	do.	<.100	E.003	.10	<.100	<.050	<.050	<1.500	<2.000	<.090
CA03	08-16-00	1700	do.	E.2	E.1	.66	<.220	<.060	<.070	<2.000	<2.500	<.090
CA04	08-09-00	1700	do.	E.3	<.200	.21	<.220	<.060	<.070	<2.000	<2.500	E.08
CA05	04-15-99	1700	do.	--	--	--	--	--	--	--	--	--
CA06	04-11-99	0715	do.	<.100	<.200	--	<.100	<.050	<.050	<1.500	E6	.17
CA07	09-21-99	1110	do.	<.100	<.200	--	<.150	<.050	<.050	<.900	<1.500	E.04
CA08	09-21-99	1600	do.	<.100	<.200	--	<.150	<.050	<.050	<.900	<1.500	<.090
CA09	09-22-99	1120	do.	<.100	<.200	--	<.150	<.050	<.050	<.900	<1.500	E.06
CA10	09-22-99	1320	do.	<.100	<.200	--	<.150	<.050	<.050	<.900	<1.500	<.090
CO01	04-21-99	1250	do.	E2	E1	--	.41	<.050	<.050	<1.500	E8	E.7
DE01	05-23-99	1130	do.	E.1	E.04	--	<.100	<.050	<.050	<1.500	<2.000	<.090
DE01	05-23-99	1140	duplicate	<.100	E.04	--	<.100	<.050	<.050	<1.500	E2	<.090
FL01	08-28-00	1215	do.	E.09	<.200	<.150	<.220	<.060	<.070	<2.000	<2.000	<.090
FL02	08-23-00	1215	do.	E.2	<.200	<.150	<.220	<.060	<.070	<2.000	<2.500	E.09
GA01	05-26-99	1400	do.	--	--	--	--	--	--	--	--	--
GA02	05-25-99	1130	do.	--	--	--	--	--	--	--	--	--
GA03	05-25-99	1030	do.	--	--	--	--	--	--	--	--	--
GA04	05-25-99	0840	do.	E.1	E.04	--	<.100	<.060	<.050	E2	E10	E.05
GA05	05-26-99	1130	do.	--	--	--	--	--	--	--	--	--
GA06	05-24-99	1215	do.	--	--	--	--	--	--	--	--	--
GA07	05-31-00	1115	do.	E.1	E.05	<.100	<.100	<.050	<.050	<1.500	<2.000	.23
IA01	09-13-00	1600	do.	<.100	<.200	<.100	<.150	<.050	<.050	<2.000	E10	<.090
IA02	09-12-00	1200	do.	<.100	<.200	<.100	<.220	<.050	<.050	<2.000	<2.500	<.090
IA04	09-11-00	1700	do.	E.06	<.200	<.100	<.150	<.050	<.050	<2.000	<2.500	<.090
IA05	04-05-99	1445	do.	--	--	--	--	--	--	--	--	--
IA07	04-08-99	1000	do.	--	--	--	--	--	--	--	--	--
IA08	04-06-99	0935	do.	--	--	--	--	--	--	--	--	--
IA09	04-06-99	1245	do.	E.08	E.03	--	<.100	<.050	<.05