Emerging Contaminants in the Environment Investigations — Analytical Methods Development

A

Alvarez, D.A., Stackelberg, P.E., Petty, J.D., Huckins, J.N., Furlong, E.T., Zaugg, S.D., and Meyer, M.T., 2005,

Comparison of a novel passive sampler to standard water-column sampling for organic contaminants associated with wastewater effluents entering a New Jersey stream: Chemosphere, v. 61, no. 5, p. 610-622, doi:10.1016/j.chemosphere.2005.03.023.

B

Burkhardt, M.R., ReVello, R.C., Smith, S.G., and Zaugg, s.D., 2005,

Pressurized liquid extraction using water/isopropanol coupled with solid-phase extraction cleanup for industrial and anthropogenic waste-indicator compounds in sediment: Analytica Chimica Acta, v. 534, no. 1, p. 89-100, doi:10.1016/j.aca.2004.11.023.

Burkhardt, M.R., Zaugg, S.D., Smith, S.G., and ReVello, R.C., 2006,

Determination of wastewater compounds in sediment and soil by pressurized solvent extraction, solid-phase extraction, and capillary-column gas chromatography/mass spectrometry: U.S. Geological Survey Techniques and Methods, book 5, sec. B, chap. 2, 33 p.

C

Cahill, J.D., Furlong, E.T., Burkhardt, M.R., Kolpin, D.W., and Anderson, L.G., 2004,

Determination of pharmaceutical compounds in surface- and ground-water samples by solid-phase extraction and high-performance liquid chromatography--electrospray ionization mass spectrometry: Journal of Chromatography A, v. 1041, no. 1-2, p. 171-180, doi:10.1016/j.chroma.2004.04.005.

E

Eganhouse, R.P., Pontolillo, J., Gaines, R.B., Frysinger, G.S., Gabriel, F.L.P., Kohler, H.-P.E., Giger, W., and Barber, L.B., 2009,

Isomer-specific determination of 4-nonylphenols using comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry: Environmental Science and Technology, v. 43, no. 24, p. 9306-9313, doi:10.1021/es902622r.

F

Ferrer, I., Barber, L.B., and Thurman, E.M., 2009,

Gas chromatographic-mass spectrometric fragmentation study of phytoestrogens as their trimethylsilyl derivatives--Identification in soy milk and wastewater samples: Journal of Chromatography A, v. 1216, no. 32, p. 6024-6032, doi:10.1016/j.chroma.2009.06.042.

Furlong, E.T., Werner, S.L., Anderson, B.D., and Cahill, J.D., 2008,

Determination of human-health pharmaceuticals in filtered water by chemically modified styrene-divinylbenzene resin-based solid-phase extraction and high-performance liquid chromatography/mass spectrometry: U.S. Geological Survey Techniques and Methods book 5, sec. B, chap. B5, 56 p.

G

Graham, J.L., Loftin, K.A., Ziegler, A.C., and Meyer, M.T., 2008,

Cyanobacteria in lakes and reserviors--Toxin and taste-and-odor sampling guidelines (ver. 1.0): U.S. Geological Survey Techniques of Water-Resources Investigations, book 9, chap. A7, section 7.5, 65 p (available online only).

Graham, J.L., Loftin, K.A., Ziegler, A.C., and Meyer, M.T., 2008,

Guidelines for design and sampling for cyanobacterial toxin and taste-and-odor studies in lakes and reservoirs: U.S. Geological Survey Scientific Investigations Report 2008-5038, 39 p.

H

Haack, S.K., Duris, J.W., Fogarty, L.R., Kolpin, D.W., Focazio, M.J., Furlong, E.T., and Meyer, M.T., 2009,

Comparing wastewater chemicals, indicator bacteria concentrations, and bacterial pathogen genes as fecal pollution indicators: Journal of Environmental Quality, v. 38, no. 1, p. 248-258, doi:10.2134/jeq2008.0173.

K

Kinney, C.A., Furlong, E.T., Werner, S.L., and Cahill, J.D., 2006,

Presence and distribution of wastewater-derived pharmaceuticals in soil irrigated with reclaimed water: Environmental Toxicology and Chemistry, v. 25, no. 2, p. 317-326, doi:10.1897/05-187R.1.

Kinney, C.A., Furlong, E.T., Zaugg, S.D., Burkhardt, M.R., Werner, S.L., Cahill, J.D., and Jorgensen, G.R., 2006,

Survey of organic wastewater contaminants in biosolids destined for land application: Environmental Science and Technology, v. 40, no. 23, p. 7207-7215, doi:10.1021/es0603406.

L

Leenheer, J.A., and Rostad, C.E., 2004,

Fractionation and characterization of organic matter in wastewater from a swine waste-retention basin: U.S. Geological Survey Scientific Investigations Report 2004-5217, 21 p.

Lindsey, M.E., Meyer, M.T., and Thurman, E.M., 2001,

Analysis of trace levels of sulfonamide and tetracycline antimicrobials in groundwater and surface water using solid-phase extraction and liquid chromatography/mass spectrometry: Analytical Chemistry, v. 73, no. 19, p. 4640-4646, doi:10.1021/ac010514w.

Loftin, K.A., Meyer, M.T., Rubio, F., Kamp, L., Humphries, E., and Whereat, E., 2008,

Comparison of two cell lysis procedures for recovery of microcystins in water samples from Silver Lake in Dover, Delaware, with microcystin producing cyanobacterial accumulations: U.S. Geological Survey Open-File Report 2008-1341, 9 p.

Loper, C.A., Crawford, J.K., Otto, K.L., Manning, R.L., Meyer, M.T., and Furlong, E.T., 2007,

Concentrations of selected pharmaceuticals and antibiotics in south-central Pennsylvania waters, March through September 2006: U.S. Geological Survey Data Series 300, 101 p.

M

Meyer, M.T., Lee, E.A., Ferrell, G.F., Bumgarner, J.E., and Varnes, J., 2007,

Evaluation of tandem off-line and on-line solid-phase extraction with liquid chromatography/electrospray ionization-mass spectrometry for the analysis of antibiotics in ambient water and comparision to an independent method: U.S. Geological Survey Scientific Investigations Report 2007-5021, 28 p.

P

Phillips, P.J., Smith, S.G., Kolpin, D.W., Zaugg, S.D., Buxton, H.T., Furlong, E.T., Esposito, K., and Stinson, B., 2010,

Method description, quality assurance, environmental data, and other information for analysis of pharmaceuticals in wastewater-treatment-plant effluents, stream water, and reservoirs, 2004-2009: U.S. Geological Survey Open-File Report 2010-1102.

R

Rosen, B.H., Loftin, K.A., Smith, C.E., Lane, R.F., and Keydel, S.P., 2010,

Microphotographs of cyanobacteria documenting the effects of various cell-lysis techniques: U.S. Geological Survey Open-File Report 2010-1289, 203 p.

S

Schultz, M.M., and Furlong, E.T., 2008,

Trace analysis of antidepressant pharmaceuticals and their select degradates in aquatic matrixes by LC/ESI/MS/MS: Analytical Chemistry, v. 80, no. 5, p. 1756-1762, doi:10.1021/ac702154e.

W

Writer, J.H., Keefe, S.K., Ryan, J.N., Ferrer, I., Thurman, M.E., and Barber, L.B., 2011,

Methods for evaluating in-stream attenuation of trace organic compounds: Applied Geochemistry, v. 26, Supplement, p. S344-S345, doi:10.1016/j.apgeochem.2011.03.071.

Y

Ye, Z., Weinberg, H.S., and Meyer, M.T., 2007,

Trace analysis of trimethoprim and sulfonamide, macrolide, quinolone, and tetracycline antibiotics in chlorinated drinking water using liquid chromotagrphy electrospray tandem mass spectrometry: Analytical Chemistry, v. 79, no. 3, p. 1135-1144, doi:10.1021/ac060972a.

Z

Zaugg, S.D., Burkhardt, M.R., Burbank, T.L., Olson, M.C., Iverson, J.L., and Schroeder, M.P., 2006,

Determination of semivolatile organic compounds and polycyclic aromatic hydrocarbons in solids by gas chromatography/mass spectrometry: U.S. Geological Survey Techniques and Methods, book 5, sec. B, chap. 3, 44 p.

Zaugg, S.D., Smith, S.G., and Schroeder, M.P., 2006,

Determination of wastewater compounds in whole water by continuous liquid-liquid extraction and capillary-column gas chromatography/mass spectrometry: U.S. Geological Survey Techniques and Methods, book 5, sec, B, chap. 4, 30 p.

Zaugg, S.D., Smith, S.G., Schroeder, M.P., Barber, L.B., and Burkhardt, M.R., 2002,

Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory--Determination of wastewater compounds by polystyrene-divinylbenzene solid-phase extraction and capillary-column gas chromatography/mass spectrometry: U.S. Geological Survey Water-Resources Investigations Report 01-4186, 37 p.

Zimmerman, L.R., Strahan, A.P., and Thurman, E.M., 2001,

Method of analysis and quality-assurance practices by the U.S. Geological Survey Organic Geochemistry Research Group--Determination of four selected mosquito insecticides and a synergist in water using liquid-liquid extraction and gas chromatography/mass spectrometry: U.S. Geological Survey Open-File Report 01-273, 11 p.

Zimmerman, L.R., Ziegler, A.C., and Thurman, E.M., 2002,

Method of analysis and quality-assurance practices by U.S. Geological Survey Organic Geochemistry Research Group--Determination of geosmin and methylisoborneol in water using solid-phase microextraction and gas chromatography/mass spectrometry: U.S. Geological Survey Open-File Report 02-337, 12 p.

There are 27 on-line publications in this section of the bibliography. The Toxics Bibliographic Data Base was last updated on 2/8/12.

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